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These materials crystallize in a Hexagonal Close Packed (HCP) structure with a c/a ratio greater than 1.67 which results in kink band formations when subjected to loading. The stress-strain responses of these materials are characterized by a rate and temperature dependent hysteresis. In this work, we report the microstructural changes associated with thermal shocking of Mn+1AXn phases and its effects on deformation mechanisms, under compressive loading at high strain rates using a Split Hopkinson Pressure Bar (SHPB). The specimens are heated to temperatures of 220, 550 and 900oC, held at each temperature for 5-10 minutes, and subsequently quenched in water at 20oC to induce thermal shock. The thermal shock resistance and its effect on mechanical properties is investigated by subjecting heat treated specimens to compressive loading at high strain rates (~1000-4500 s-1) using a Split Hopkinson Pressure Bar (SHPB). The microstructures of thermally shocked specimens are characterized by Scanning Electron Microscopy (SEM) combined with Energy Dispersive Spectroscopy (EDS) analysis to reveal the surface morphologies and characteristics. The displacements during mechanical characterization by SHPB are measured using a high speed, full-field 2D Digital Image Correlation (DIC) technique followed by microstructural analysis of deformed/fractured specimen for studying microscale mechanisms associated with deformation. The results from this analysis are used to validate a mechanism based constitutive model, developed by the authors, for temperature and rate dependent hysteresis in Mn+1AXn phase materials.", "proceedingsTitle": "Proceedings of the ASME 2012 International Mechanical Engineering Congress and Exposition (IMECE2012)", "conferenceName": "International Mechanical Engineering Congress and Exposition (IMECE2012)", "publisher": "ASME", "place": "Houston, Texas", "date": "9-15 November 2012", "eventPlace": "", "volume": "", "issue": "", "numberOfVolumes": "", "pages": "", "series": "", "seriesNumber": "", "DOI": "", "ISBN": "", "citationKey": "", "url": "", "accessDate": "", "ISSN": "", "archive": "", "archiveLocation": "", "shortTitle": "", "language": "", "libraryCatalog": "", "callNumber": "", "rights": "", "extra": "", "tags": [], "collections": [ "DX4GZADC" ], "relations": {}, "dateAdded": "2013-01-11T19:16:21Z", "dateModified": "2013-01-11T19:16:21Z" } }, { "key": "AJAZ9SF9", "version": 2, "library": { "type": "group", "id": 88191, "name": "SMRL", "links": { "alternate": { "href": "https://www.zotero.org/groups/smrl", "type": "text/html" } } }, "links": { "self": { "href": "https://api.zotero.org/groups/88191/items/AJAZ9SF9", "type": "application/json" }, "alternate": { "href": "https://www.zotero.org/groups/smrl/items/AJAZ9SF9", "type": "text/html" }, "up": { "href": "https://api.zotero.org/groups/88191/items/8TDIJR5B", "type": "application/json" } }, "meta": { "createdByUser": { "id": 603384, "username": "jacob.davidson", "name": "Jacob Davidson", "links": { "alternate": { "href": "https://www.zotero.org/jacob.davidson", "type": "text/html" } } }, "numChildren": 0 }, "data": { "key": "AJAZ9SF9", "version": 2, "parentItem": "8TDIJR5B", "itemType": "attachment", "linkMode": "imported_file", "title": "Davidson and Goulbourne - 2012 - Connecting chain chemistry and network topology wi.pdf", "accessDate": "", "url": "", "note": "", "contentType": "application/pdf", "charset": "", "filename": "Davidson and Goulbourne - 2012 - Connecting chain chemistry and network topology wi.pdf", "md5": "5834e653927ec323a5da081adc832aee", "mtime": 1357930652000, "tags": [], "relations": {}, "dateAdded": "2013-01-11T18:57:32Z", "dateModified": "2013-01-11T18:57:32Z" } }, { "key": "8TDIJR5B", "version": 1, "library": { "type": "group", "id": 88191, "name": "SMRL", "links": { "alternate": { "href": "https://www.zotero.org/groups/smrl", "type": "text/html" } } }, "links": { "self": { "href": "https://api.zotero.org/groups/88191/items/8TDIJR5B", "type": "application/json" }, "alternate": { "href": "https://www.zotero.org/groups/smrl/items/8TDIJR5B", "type": "text/html" } }, "meta": { "createdByUser": { "id": 603384, "username": "jacob.davidson", "name": "Jacob Davidson", "links": { "alternate": { "href": "https://www.zotero.org/jacob.davidson", "type": "text/html" } } }, "creatorSummary": "Davidson and Goulbourne", "parsedDate": "2012", "numChildren": 1 }, "data": { "key": "8TDIJR5B", "version": 1, "itemType": "conferencePaper", "title": "Connecting chain chemistry and network topology with the large deformation mechanical response of elastomers", "creators": [ { "creatorType": "author", "firstName": "Jacob D.", "lastName": "Davidson" }, { "creatorType": "author", "firstName": "N. 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C.", "lastName": "Goulbourne" }, { "creatorType": "editor", "firstName": "Tom", "lastName": "Proulx" } ], "abstractNote": "Soft polymers are widely used as interlayers and adhesives in multi-layered systems for defense applications. This research focuses on the large deformation response of several polyacrylate adhesives with varying microstructures. Understanding the mechanical response of these materials under numerous dynamic loading conditions is instrumental in deriving high fidelity constitutive models and optimizing performance when integrated into a multi-layered structure. In recent years, there has been an emphasis on rate dependence research of soft materials, such as thermoplastic polyurethanes/polyureas (moduli order of 3–5 MPa), at quasi-static and very high rates (SHPB), but not intermediate. The goal is to characterize ultra-soft polyacrylates (moduli on the order of 100–600 kPa) through a wide range of strain rates (0.001–1 /s) using different methods and modes of loading. Methods utilized are Instron (servohydraulic and ElectroPULS) tensile and compression testing, and intermediate instrumented impact on multi-laminates. Characteristics of the large, non-linear deformation testing response include: rate dependence, hysteresis, cyclic effects and strain softening. The microstructure and mechanical behavior of the polyacrylate adhesives is related to the capability to modulate impact loads for loading times of approximately 2 milliseconds.", "bookTitle": "Time Dependent Constitutive Behavior and Fracture/Failure Processes, Volume 3", "series": "Conference Proceedings of the Society for Experimental Mechanics Series", "seriesNumber": "15", "volume": "", "numberOfVolumes": "", "edition": "", "date": "2011/01/01", "publisher": "Springer New York", "place": "", "originalDate": "", "originalPublisher": "", "originalPlace": "", "format": "", "pages": "241-258", "ISBN": "978-1-4419-9498-1, 978-1-4419-9794-4", "DOI": "", "citationKey": "", "url": "http://link.springer.com.proxy.lib.umich.edu/chapter/10.1007/978-1-4419-9794-4_35", "accessDate": "2013-01-11T18:21:37Z", "ISSN": "", "archive": "", "archiveLocation": "", "shortTitle": "", "language": "en", "libraryCatalog": "link.springer.com.proxy.lib.umich.edu", "callNumber": "", "rights": "©2011 The Society for Experimental Mechanics, Inc.", "extra": "", "tags": [ { "tag": "Materials Science, general", "type": 1 }, { "tag": "Mechanics", "type": 1 }, { "tag": "Theoretical and Applied Mechanics", "type": 1 } ], "collections": [ "I2N3858X" ], "relations": {}, "dateAdded": "2013-01-11T18:21:37Z", "dateModified": "2013-01-11T18:21:37Z" } }, { "key": "4H7HWQD9", "version": 2, "library": { "type": "group", "id": 88191, "name": "SMRL", "links": { "alternate": { "href": "https://www.zotero.org/groups/smrl", "type": "text/html" } } }, "links": { "self": { "href": "https://api.zotero.org/groups/88191/items/4H7HWQD9", "type": "application/json" }, "alternate": { "href": "https://www.zotero.org/groups/smrl/items/4H7HWQD9", "type": "text/html" } }, "meta": { "createdByUser": { "id": 603384, "username": "jacob.davidson", "name": "Jacob Davidson", "links": { "alternate": { "href": "https://www.zotero.org/jacob.davidson", "type": "text/html" } } }, "creatorSummary": "Goulbourne et al.", "parsedDate": "2008", "numChildren": 0 }, "data": { "key": "4H7HWQD9", "version": 2, "itemType": "bookSection", "title": "Modeling Dielectric Elastomer Membranes", "creators": [ { "creatorType": "author", "firstName": "N. C.", "lastName": "Goulbourne" }, { "creatorType": "author", "firstName": "E. M.", "lastName": "Mockensturm" }, { "creatorType": "author", "firstName": "M.", "lastName": "Frecker" } ], "abstractNote": "", "bookTitle": "Dielectric Elastomers as Electromechanical Transducers", "series": "", "seriesNumber": "", "volume": "", "numberOfVolumes": "", "edition": "", "date": "2008", "publisher": "Elsevier", "place": "", "originalDate": "", "originalPublisher": "", "originalPlace": "", "format": "", "pages": "", "ISBN": "", "DOI": "", "citationKey": "", "url": "", "accessDate": "", "ISSN": "", "archive": "", "archiveLocation": "", "shortTitle": "", "language": "", "libraryCatalog": "", "callNumber": "", "rights": "", "extra": "", "tags": [], "collections": [ "I2N3858X" ], "relations": {}, "dateAdded": "2013-01-11T18:18:54Z", "dateModified": "2013-01-11T18:20:51Z" } }, { "key": "JTJCS2QT", "version": 3, "library": { "type": "group", "id": 88191, "name": "SMRL", "links": { "alternate": { "href": "https://www.zotero.org/groups/smrl", "type": "text/html" } } }, "links": { "self": { "href": "https://api.zotero.org/groups/88191/items/JTJCS2QT", "type": "application/json" }, "alternate": { "href": "https://www.zotero.org/groups/smrl/items/JTJCS2QT", "type": "text/html" }, "up": { "href": "https://api.zotero.org/groups/88191/items/747IB3TG", "type": "application/json" } }, "meta": { "createdByUser": { "id": 603384, "username": "jacob.davidson", "name": "Jacob Davidson", "links": { "alternate": { "href": "https://www.zotero.org/jacob.davidson", "type": "text/html" } } }, "numChildren": 0 }, "data": { "key": "JTJCS2QT", "version": 3, "parentItem": "747IB3TG", "itemType": "attachment", "linkMode": "imported_url", "title": "Son_Seyul_D_2011.pdf", "accessDate": "2012-12-09T21:19:18Z", "url": "http://scholar.lib.vt.edu/theses/available/etd-08092011-133217/unrestricted/Son_Seyul_D_2011.pdf", "note": "", "contentType": "application/pdf", "charset": "", "filename": "Son_Seyul_D_2011.pdf", "md5": "d05863acb27cd1f2ed228b95780154d9", "mtime": 1355087961000, "tags": [], "relations": { "owl:sameAs": "http://zotero.org/groups/131243/items/BPTE95CB" }, "dateAdded": "2012-12-09T21:19:18Z", "dateModified": "2012-12-09T21:20:20Z" } }, { "key": "MJZQR35Z", "version": 1, "library": { "type": "group", "id": 88191, "name": "SMRL", "links": { "alternate": { "href": "https://www.zotero.org/groups/smrl", "type": "text/html" } } }, "links": { "self": { "href": "https://api.zotero.org/groups/88191/items/MJZQR35Z", "type": "application/json" }, "alternate": { "href": "https://www.zotero.org/groups/smrl/items/MJZQR35Z", "type": "text/html" } }, "meta": { "createdByUser": { "id": 603384, "username": "jacob.davidson", "name": "Jacob Davidson", "links": { "alternate": { "href": "https://www.zotero.org/jacob.davidson", "type": "text/html" } } }, "creatorSummary": "Goulbourne et al.", "parsedDate": "2003", "numChildren": 0 }, "data": { "key": "MJZQR35Z", "version": 1, "itemType": "conferencePaper", "title": "Modeling of a dielectric elastomer diaphragm for a prosthetic blood pump", "creators": [ { "creatorType": "author", "firstName": "N.", "lastName": "Goulbourne" }, { "creatorType": "author", "firstName": "M. I.", "lastName": "Frecker" }, { "creatorType": "author", "firstName": "E. M.", "lastName": "Mockensturm" }, { "creatorType": "author", "firstName": "A. 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